cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane

Base Information

• Chemical Name: cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane
• CAS No.: 102987-41-7
• Molecular Formula: C₁₂H₁₈O₂P₂
• Molecular Weight: 256.221
• Mol file: 102987-41-7.mol

Synonyms:cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane

Chemical Property of cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane

There total 1 articles about cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

bis(hydroxymethyl)phenylphosphine (3127-08-0) + tert-butyldichlorophosphine (25979-07-1) → cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane (102987-41-7)

Guidance literature:

With triethylamine; In benzene;

DOI:10.1007/BF01171046

Reference yield: 90.0%

cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane (102987-41-7) → 2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane 2,5-disulfide

Guidance literature:

With sulfur; In benzene; for 0.166667h; Heating;

DOI:10.1007/BF01171046

Reference yield: 80.0%

cis-2-tert-butyl-5-phenyl-1,3,2,5-dioxadiphosphorinane (102987-41-7) → 2-tert-Butyl-5-phenyl-[1,3,2,5]dioxadiphosphinane 2,5-diselenide

Guidance literature:

With selenium; In benzene; for 1h; Heating;

DOI:10.1007/BF01171046

upstream raw materials:

bis(hydroxymethyl)phenylphosphine

tert-butyldichlorophosphine