methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

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Chemical Name:methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt
CAS No.:1448711-05-4
Molecular Formula:C₂₂H₃₁N₂O₁₀*Na
Molecular Weight:506.485
Hs Code.:

Synonyms:methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

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Chemical Property of methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

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Technology Process of methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

There total 2 articles about methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1448711-03-2
C₂₉H₄₀N₂O₁₃

: 1448711-05-4
methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 1.5h;
DOI:10.1002/anie.201207267

Reference yield:

: 5139-89-9
4-phenoxybutyryl chloride

: C₁₉H₃₀N₂O₁₁

: 1448711-05-4
methyl 5-acetamido-4-phenoxybutyrylamido-3,4,5-trideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: sodium hydroxide / methanol / 1.5 h / 20 °C

With triethylamine; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1002/anie.201207267