Technology Process of 3-benzyl-1-ethylaluminacyclopentane
There total 1 articles about 3-benzyl-1-ethylaluminacyclopentane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
zirconocene dichloride;
under Ar; allylbenzene was added to a mixture of Cp2ZrCl2 and Et3Al; stirred for 10 h at 23-25°C; (13)C-NMR;
DOI:10.1007/BF01184540
- Guidance literature:
-
3-benzyl-1-ethylaluminacyclopentane;
With
phosphorus trichloride;
In
dichloromethane;
at -10 - 20 ℃;
for 6h;
Inert atmosphere;
With
water;
In
dichloromethane;
Reagent/catalyst;
Acidic conditions;
DOI:10.1016/j.mencom.2017.01.006
- Guidance literature:
-
3-benzyl-1-ethylaluminacyclopentane; triethylaluminum;
With
phosphorus trichloride;
In
dichloromethane;
at -10 - 20 ℃;
for 6h;
Inert atmosphere;
With
water;
In
dichloromethane;
Reagent/catalyst;
Acidic conditions;
DOI:10.1016/j.mencom.2017.01.006
