2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl

Base Information

• Chemical Name: 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl
• CAS No.: 477801-25-5
• Molecular Formula: C₆F₄IN
• Molecular Weight: 288.971
• Mol file: 477801-25-5.mol

Synonyms:2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl

Chemical Property of 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl

There total 3 articles about 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,5,6-tetrafluoro-4-iodo-phenyl azide (477801-24-4) → 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl (477801-25-5)

Guidance literature:

In various solvent(s); at -270.15 ℃; UV-irradiation;

DOI:10.1002/1521-3773(20020802)41:15<2742::AID-ANIE2742>3.0.CO;2-U

Reference yield:

2,3,5,6-tetrafluoroaniline (700-17-4) → 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl (477801-25-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 72 percent / yellow HgO; iodine / ethanol

2.1: trifluoroacetic acid; sodium nitrite / H₂O / 0.25 h / 0 °C

2.2: 67 percent / sodium azide / H₂O / 1 h / 20 °C

3.1: various solvent(s) / -270.15 °C / UV-irradiation

With iodine; trifluoroacetic acid; mercury(II) oxide; sodium nitrite; In ethanol; water;

DOI:10.1002/1521-3773(20020802)41:15<2742::AID-ANIE2742>3.0.CO;2-U

Reference yield:

4-iodo-2, 3, 5, 6-tetrafluoroaniline (1991-43-1) → 2,3,5,6-tetrafluoro-4-iodo-phenylnitrenyl (477801-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid; sodium nitrite / H₂O / 0.25 h / 0 °C

1.2: 67 percent / sodium azide / H₂O / 1 h / 20 °C

2.1: various solvent(s) / -270.15 °C / UV-irradiation

With trifluoroacetic acid; sodium nitrite; In water;

DOI:10.1002/1521-3773(20020802)41:15<2742::AID-ANIE2742>3.0.CO;2-U

upstream raw materials:

2,3,5,6-tetrafluoro-4-iodo-phenyl azide

2,3,5,6-tetrafluoroaniline

4-iodo-2, 3, 5, 6-tetrafluoroaniline