N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

Base Information

Chemical Name:N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine
CAS No.:944282-46-6
Molecular Formula:C₂₄H₂₄N₂O₄S
Molecular Weight:436.532
Hs Code.:

Synonyms:N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

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Chemical Property of N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

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Technology Process of N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

There total 8 articles about N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 944282-06-8
2-(2-benzothienyl)-3-oxa-1-azaspiro[4.5]dec-1-en-4-one

: 2935-35-5
(S)-2-phenylglycine

: 944282-46-6
N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

Guidance literature:: 2-(2-benzothienyl)-3-oxa-1-azaspiro[4.5]dec-1-en-4-one; (S)-2-phenylglycine; With 4-methyl-morpholine; Heating / reflux;

With potassium hydrogensulfate; In water;

Reference yield: 34.0%

: 2-(2-benzothienyl)-3-oxa-1-azaspiro[4.5]dec-1-en-4-one

: 2935-35-5
(S)-2-phenylglycine

: 944282-46-6
N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

Guidance literature:: 2-(2-benzothienyl)-3-oxa-1-azaspiro[4.5]dec-1-en-4-one; (S)-2-phenylglycine; With 4-methyl-morpholine; Heating / reflux;

With potassium hydrogensulfate; In water;

Reference yield:

: 1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid

: 944282-46-6
N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C

2: 4-methyl-morpholine / Heating / reflux

With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;