Technology Process of C42H34N2O12S2
There total 4 articles about C42H34N2O12S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / K2CO3 / acetonitrile
2: 70 percent / NaNO3, HCl, Ac2O / CH2Cl2
3: 85 percent / NaH / tetrahydrofuran
4: 1.) Me3SiI, 2.) aq. Na2S2O3
With
hydrogenchloride; sodium nitrate; trimethylsilyl iodide; acetic anhydride; sodium hydride; potassium carbonate; sodium thiosulfate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/cc9960002161
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / NaNO3, HCl, Ac2O / CH2Cl2
2: 85 percent / NaH / tetrahydrofuran
3: 1.) Me3SiI, 2.) aq. Na2S2O3
With
hydrogenchloride; sodium nitrate; trimethylsilyl iodide; acetic anhydride; sodium hydride; sodium thiosulfate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/cc9960002161
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / NaH / tetrahydrofuran
2: 1.) Me3SiI, 2.) aq. Na2S2O3
With
trimethylsilyl iodide; sodium hydride; sodium thiosulfate;
In
tetrahydrofuran;
DOI:10.1039/cc9960002161