1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

Base Information

Chemical Name:1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane
CAS No.:73200-40-5
Molecular Formula:C₂₃H₃₀Cl₃NO₅S
Molecular Weight:538.92
Hs Code.:

Synonyms:1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

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Chemical Property of 1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

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Technology Process of 1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

There total 7 articles about 1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 73200-39-2
1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanoyl>azacyclopentane

: 73200-40-5
1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

Guidance literature:: With diphosphorus pentasulfide; triethylamine; In dichloromethane;
DOI:10.1021/jo01298a022

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 73200-40-5
1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / benzene

2: oxalyl chloride, Me₂SO, triethylamine

3: magnesium, water

4: 87 percent / pyridine / CH₂Cl₂ / 1.) addition over 2 min, -78 deg C, 2.) 0 deg C, 2.5 h

5: 1.) hydrochloric acid, 2.) water

6: 95 percent / pyridine / CH₂Cl₂

7: 75 percent / phosphorus pentasulfide, triethylamine / CH₂Cl₂

With pyridine; hydrogenchloride; diphosphorus pentasulfide; oxalyl dichloride; water; magnesium; dimethyl sulfoxide; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo01298a022

Reference yield:

: 73200-35-8
5-hydroxy-1-(pyrrolidin-1-yl)pentan-1-one

: 73200-40-5
1-<9-Benzoyloxy-5-<(2,2,2-trichloroethoxy)formyloxy>nonanethioyl>azacyclopentane

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl chloride, Me₂SO, triethylamine

2: magnesium, water

3: 87 percent / pyridine / CH₂Cl₂ / 1.) addition over 2 min, -78 deg C, 2.) 0 deg C, 2.5 h

4: 1.) hydrochloric acid, 2.) water

5: 95 percent / pyridine / CH₂Cl₂

6: 75 percent / phosphorus pentasulfide, triethylamine / CH₂Cl₂

With pyridine; hydrogenchloride; diphosphorus pentasulfide; oxalyl dichloride; water; magnesium; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1021/jo01298a022