cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

Base Information

Chemical Name:cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one
CAS No.:82679-60-5
Molecular Formula:C₂₂H₂₂N₄O₄
Molecular Weight:406.441
Hs Code.:

Synonyms:cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

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Chemical Property of cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

Chemical Property:

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Technology Process of cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

There total 5 articles about cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis-1-(1'-benzyloxycarbonyl-2'-triphenylsilyloxypropyl)-3-azido-4-styrylazetidin-2-one

: 82679-60-5
cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

: cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; water; at 0 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4020(01)81577-5

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 82679-60-5
cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / molecular sieves / CH₂Cl₂ / a) 40 deg C, 5 min, b) room temperature, 10 h

2: triethylamine, ethyl chloroformate / CH₂Cl₂ / a) -20 deg C, 4 h, b) room temperature, overnight

3: trifluoroacetic acid / tetrahydrofuran; H₂O / 1 h / 0 °C

With molecular sieve; chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0040-4020(01)81577-5

Reference yield:

: 143000-26-4
benzyl D-threonin triphenylsilyl ether

: 82679-60-5
cis-1-(1'-benzyloxycarbonyl-2'-hydroxypropyl)-3-azido-4-styrylazetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / molecular sieves / CH₂Cl₂ / a) 40 deg C, 5 min, b) room temperature, 10 h

2: triethylamine, ethyl chloroformate / CH₂Cl₂ / a) -20 deg C, 4 h, b) room temperature, overnight

3: trifluoroacetic acid / tetrahydrofuran; H₂O / 1 h / 0 °C

With molecular sieve; chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0040-4020(01)81577-5