2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Base Information

Chemical Name:2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside
CAS No.:1384861-33-9
Molecular Formula:C₅₅H₄₆O₉
Molecular Weight:850.965
Hs Code.:

Synonyms:2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Suppliers and Price of 2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

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Chemical Property of 2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of 2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

There total 4 articles about 2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174458-38-8
2-allylphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1384861-33-9
2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / 20 °C / pH 9

1.2: Dowex Monosphere 650C

2.1: pyridine / 16 h

2.2: 3 h / 20 °C

With pyridine; sodium methylate; In methanol;
DOI:10.3762/bjoc.8.66

Reference yield:

: 1745-81-9
o-Allylphenol

: 1384861-33-9
2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate; triethylamine / dichloromethane / 16 h / 20 °C

2.1: sodium methylate / methanol / 1 h / 20 °C / pH 9

2.2: Dowex Monosphere 650C

3.1: pyridine / 16 h

3.2: 3 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; sodium methylate; triethylamine; In methanol; dichloromethane;
DOI:10.3762/bjoc.8.66

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1384861-33-9
2-allylphenyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate; triethylamine / dichloromethane / 16 h / 20 °C

2.1: sodium methylate / methanol / 1 h / 20 °C / pH 9

2.2: Dowex Monosphere 650C

3.1: pyridine / 16 h

3.2: 3 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; sodium methylate; triethylamine; In methanol; dichloromethane;
DOI:10.3762/bjoc.8.66