(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

Base Information

Chemical Name:(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal
CAS No.:875438-89-4
Molecular Formula:C₁₉H₂₉NO₃S
Molecular Weight:351.51
Hs Code.:

Synonyms:(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

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Technology Process of (3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

There total 5 articles about (3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 875438-84-9
(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentionitrile

: 875438-89-4
(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃;
DOI:10.1039/b808644c

Reference yield:

: 875438-80-5
(3R)-(p-toluenesulfonyl)amino-4,4-dimethylpentonitrile

: 875438-89-4
(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

Guidance literature:: Multi-step reaction with 2 steps

1: Cs₂CO₃ / acetonitrile / 25 °C

2: Dibal-H / CH₂Cl₂ / -78 °C

With diisobutylaluminium hydride; caesium carbonate; In dichloromethane; acetonitrile;
DOI:10.1039/b515547a

Reference yield:

: 216220-10-9
(S)-2-(4-methylphenylsulfonylamino)-1-(4-methylsulfonyloxy)-3,3-dimethylbutane

: 875438-89-4
(3R)-[N-(3-methylbut-2-enyl)-N-(p-toluenesulfonyl)amino]-4,4-dimethylpentanal

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 25 °C

2: Cs₂CO₃ / acetonitrile / 25 °C

3: Dibal-H / CH₂Cl₂ / -78 °C

With diisobutylaluminium hydride; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b515547a