C₃₂H₂₆Br₂ClNO₃

Base Information

Chemical Name:C₃₂H₂₆Br₂ClNO₃
CAS No.:683813-75-4
Molecular Formula:C₃₂H₂₆Br₂ClNO₃
Molecular Weight:667.824
Hs Code.:

C<sub>32</sub>H<sub>26</sub>Br<sub>2</sub>ClNO<sub>3</sub>

Synonyms:C₃₂H₂₆Br₂ClNO₃

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Chemical Property of C₃₂H₂₆Br₂ClNO₃

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Technology Process of C₃₂H₂₆Br₂ClNO₃

There total 1 articles about C₃₂H₂₆Br₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 479422-24-7
methyl 4-[2-[5-chloro-(1-diphenylmethyl)-2-methyl-1H-indol-3-yl]ethoxy]benzoate

: 683813-75-4
C₃₂H₂₆Br₂ClNO₃

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 2.5h; Heating;
DOI:10.1021/jm061131z

Reference yield: 100.0%

: 683813-75-4
C₃₂H₂₆Br₂ClNO₃

: 479422-26-9
methyl 4-{2-[5-chloro-1-(diphenylmethyl)-2-formyl-1H-indol-3-yl]ethoxy}benzoate

Guidance literature:: C₃₂H₂₆Br₂ClNO₃; With dimethyl sulfoxide; at 20 ℃; for 0.5h; Heating / reflux;

With water;

Reference yield:

: 683813-75-4
C₃₂H₂₆Br₂ClNO₃

: 4-{2-[2-{3-[(benzylsulfonyl)amino]propyl}-5-chloro-1-(diphenylmethyl)-1H-indol-3-yl]ethoxy}benzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1.1: 0.750 g / Ag₂CO₃; H₂O / acetone

2.1: 91 percent / tetrahydrofuran / 1 h

3.1: 97 percent / morpholine / Pd(PPh₃)4 / tetrahydrofuran / 4 h

4.1: 79 percent / H₂ / Pt/C / methanol / 24 h / 760.05 Torr

5.1: (COCl)2 / CH₂Cl₂ / 1 h

5.2: 83 percent / Zn(BH₄)2; TMEDA / diethyl ether / 0.25 h

6.1: 86 percent / CBr₄; PS-PPh₃ / CH₂Cl₂ / 2 h

7.1: NaH / dimethylformamide / 0.5 h

7.2: 17 percent / dimethylformamide / 1 h

8.1: 80 percent / aq. NaOH / tetrahydrofuran; methanol / 50 °C

With morpholine; sodium hydroxide; oxalyl dichloride; PS-PPh₃; carbon tetrabromide; water; hydrogen; sodium hydride; silver carbonate; platinum on activated charcoal; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm061131z