(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

Base Information

Chemical Name:(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis
CAS No.:165054-82-0
Molecular Formula:C₃₉H₅₆O₁₇
Molecular Weight:796.863
Hs Code.:

(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis<oxy(1-methyl-3-oxopropane-1,3-diyl)>

Synonyms:(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

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Chemical Property of (R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

Chemical Property:

Purity/Quality:

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Technology Process of (R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

There total 14 articles about (R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116761-27-4
(3R)-3-<<(3'R)-3'-(benzyloxy)butanoyl>oxy>butanoic acid tert-butyl ester

: 165054-82-0
(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / H₂ / Pd/C / ethanol; acetic acid / 5 h / Ambient temperature

2: pyridine / CH₂Cl₂ / -78 °C / to RT

3: 99 percent / H₂ / Pd/C / ethyl acetate; acetic acid / Ambient temperature

4: pyridine / CH₂Cl₂ / -78 °C / to RT

5: CF₃COOH / CH₂Cl₂ / 5 h

With pyridine; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; ethyl acetate;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W

Reference yield:

: 152996-90-2
(3R)-3-<<(3'R)-3'-(benzyloxy)butanoyl>oxy>butanoic acid

: 165054-82-0
(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

Guidance literature:: Multi-step reaction with 5 steps

1: (COCl)2 / CH₂Cl₂; dimethylformamide / Ambient temperature

2: pyridine / CH₂Cl₂ / -78 °C / to RT

3: 99 percent / H₂ / Pd/C / ethyl acetate; acetic acid / Ambient temperature

4: pyridine / CH₂Cl₂ / -78 °C / to RT

5: CF₃COOH / CH₂Cl₂ / 5 h

With pyridine; oxalyl dichloride; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W

Reference yield:

: 116761-31-0
(3R)-3-<<(3'R)-3'-<<(3R)-3-<<(3'R)-3'-(benzyloxy)butyryl>oxy>butyryl>oxy>butyryl>oxy>butyric acid-(tert-butyl)ester

: 165054-82-0
(R,R,R,R,R,R,R,R)-α-benzyl-ω-hydroxyoctakis

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / Pd/C / ethyl acetate; acetic acid / Ambient temperature

2: pyridine / CH₂Cl₂ / -78 °C / to RT

3: CF₃COOH / CH₂Cl₂ / 5 h

With pyridine; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; acetic acid; ethyl acetate;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W