(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

Base Information

Chemical Name:(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone
CAS No.:1599455-14-7
Molecular Formula:C₁₈H₂₆O₂Si
Molecular Weight:302.489
Hs Code.:

Synonyms:(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

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Technology Process of (1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

There total 1 articles about (1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 5186-09-4
1-acetyl-1-benzoyl cyclopropane

: 69739-34-0
t-butyldimethylsiyl triflate

: 1599455-14-7
(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

Guidance literature:: 1-acetyl-1-benzoyl-cyclopropane; With triethylamine; In dichloromethane; at -10 ℃; for 0.333333h; Inert atmosphere;

t-butyldimethylsiyl triflate; at -10 ℃;
DOI:10.1016/j.tetlet.2014.03.035

Reference yield: 93.0%

: 1599455-14-7
(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

: 104-87-0
4-methyl-benzaldehyde

: C₂₀H₂₀O₃

Guidance literature:: (1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone; 4-methyl-benzaldehyde; With scandium tris(trifluoromethanesulfonate); In dichloromethane; at -70 - -60 ℃; for 2h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 46h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.03.035

Reference yield: 84.0%

: 1599455-14-7
(1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone

: 104-88-1
4-chlorobenzaldehyde

: C₁₉H₁₇ClO₃

Guidance literature:: (1-(1-((tert-butyldimethylsilyl)oxy)vinyl)cyclopropyl)(phenyl)methanone; 4-chlorobenzaldehyde; With scandium tris(trifluoromethanesulfonate); In dichloromethane; at -70 - -60 ℃; for 2h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 51h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.03.035