2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

Base Information

Chemical Name:2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester
CAS No.:129956-22-5
Molecular Formula:C₂₅H₃₀O₅S
Molecular Weight:442.576
Hs Code.:

Synonyms:2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

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Chemical Property of 2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

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Technology Process of 2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

There total 6 articles about 2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 133261-45-7
6-{4-[(E)-2-(4-Methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexan-1-ol

: 920-46-7,26937-45-1
Methacryloyl chloride

: 129956-22-5
2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

Guidance literature:: With N,N-dimethyl-aniline; In dichloromethane;
DOI:10.1039/c39900001093

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 129956-22-5
2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaI, 2.) aq. KOH / 1.) EtOH

2: 1.) NaH

3: 90 percent / C₆H₅NMe₂ / CH₂Cl₂

With potassium hydroxide; sodium hydride; N,N-dimethyl-aniline; sodium iodide; In dichloromethane;
DOI:10.1039/c39900001093

Reference yield:

: 96735-91-0
4-(6-hydroxyhexyl-1-oxy)benzaldehyde

: 129956-22-5
2-Methyl-acrylic acid 6-{4-[(E)-2-(4-methanesulfonyl-phenyl)-vinyl]-phenoxy}-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH

2: 90 percent / C₆H₅NMe₂ / CH₂Cl₂

With sodium hydride; N,N-dimethyl-aniline; In dichloromethane;
DOI:10.1039/c39900001093