4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

Base Information

Chemical Name:4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene
CAS No.:1300041-03-5
Molecular Formula:C₂₁H₂₂
Molecular Weight:274.406
Hs Code.:

Synonyms:4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

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Chemical Property of 4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

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Technology Process of 4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

There total 9 articles about 4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1300040-91-8
(7-methyleneoct-1-yne-1,8-diyl)dibenzene

: 1300041-03-5
4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

Guidance literature:: With trifluorormethanesulfonic acid; In 1,2-dichloro-ethane; at 80 ℃; for 9h;
DOI:10.1016/j.tetlet.2010.10.094

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 1300041-03-5
4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

Guidance literature:: Multi-step reaction with 9 steps

1.1: n-butyllithium; mercury dichloride / tetrahydrofuran / -78 - 20 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 20 °C

3.1: 1H-imidazole / tetrahydrofuran

4.1: n-butyllithium / 0 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran

6.1: dmap; triethylamine / dichloromethane

7.1: sodium iodide / acetone

8.1: copper(l) cyanide / tetrahydrofuran / -23 - 0 °C

8.2: 20 °C

9.1: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 9 h / 80 °C

With 1H-imidazole; dmap; osmium(VIII) oxide; n-butyllithium; trifluorormethanesulfonic acid; tetrabutyl ammonium fluoride; copper(l) cyanide; 4-methylmorpholine N-oxide; triethylamine; sodium iodide; mercury dichloride; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1016/j.tetlet.2010.10.094

Reference yield:

: C₁₅H₁₈O

: 1300041-03-5
4a-methyl-9-phenyl-1,2,3,4,4a,10-hexahydroanthracene

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane

2.1: sodium iodide / acetone

3.1: copper(l) cyanide / tetrahydrofuran / -23 - 0 °C

3.2: 20 °C

4.1: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 9 h / 80 °C

With dmap; trifluorormethanesulfonic acid; copper(l) cyanide; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; acetone;
DOI:10.1016/j.tetlet.2010.10.094