{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆

Base Information

• Chemical Name: {Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆
• CAS No.: 157076-97-6
• Molecular Formula: C₃₃H₄₈CuN₃P*F₆P
• Molecular Weight: 726.248

Synonyms:{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆

Chemical Property of {Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆

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Technology Process of {Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆

There total 4 articles about {Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}{P(C₆H₅)3}}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

{Cu(C6H12N3(CH(CH3)2)3)}2NO2(1+)*PF6(1-)={{Cu(C6H12N3(CH(CH3)2)3)}2NO2}PF6 (154788-34-8) + triphenylphosphine (603-35-0) → [(1,4,7-triisopropyl-1,4,7-triazacyclononane)Cu(I)(NO2)] + {Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}(1+)*PF6(1-)={{Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}}PF6 (157076-97-6)

Guidance literature:

In tetrahydrofuran; (N2); phosphine product ppt. filtered off, residue repptn. (CH2Cl2, Et2O), recrystn. (THF/pentane); elem. anal.;

DOI:10.1021/ja952691i

Reference yield: 70.0%

[(1,4,7-triisopropyl-1,4,7-triazacyclononane)Cu(CH3CN)]PF6 (154788-32-6) + triphenylphosphine (603-35-0) → {Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}(1+)*PF6(1-)={{Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}}PF6 (157076-97-6)

Guidance literature:

In tetrahydrofuran; (N2); recrystn. (CH2Cl2/Et2O); elem. anal.;

DOI:10.1021/ja952691i

Reference yield: 63.0%

{Cu(C6H12N3(CH(CH3)2)3)}2NO2(1+)*PF6(1-)={{Cu(C6H12N3(CH(CH3)2)3)}2NO2}PF6 (154788-34-8) → [(1,4,7-triisopropyl-1,4,7-triazacyclononane)Cu(I)(NO2)] + {Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}(1+)*PF6(1-)={{Cu(C6H12N3(CH(CH3)2)3)}{P(C6H5)3}}PF6 (157076-97-6)

Guidance literature:

With P(C₆H₅)3; In tetrahydrofuran; addn. of PPh3 to a soln. of the starting complex in THF; fractional crystn.;

upstream raw materials:

[(1,4,7-triisopropyl-1,4,7-triazacyclononane)Cu(CH₃CN)]PF₆

triphenylphosphine

{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}2NO₂⁽¹⁺⁾*PF₆^(1-)={{Cu(C₆H₁₂N₃(CH(CH₃)2)3)}2NO₂}PF₆

1,4,7-tri(iso-propyl)-1,4,7-triazacyclononane

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