13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

Base Information

Chemical Name:13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one
CAS No.:128404-62-6
Molecular Formula:C₂₆H₁₄N₂O₄
Molecular Weight:418.408
Hs Code.:

13-<3'-nitrobenzoyl>indeno<2,1-b>benzo<g>indolizin-12-one

Synonyms:13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

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Chemical Property of 13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

Chemical Property:

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Technology Process of 13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

There total 3 articles about 13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 119-65-3
isoquinoline

: 128404-52-4
2-hydroxy-2-<3'-nitrophenacyl>-1,3-indanedione

: 128404-62-6
13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

Guidance literature:: With p-toluenesulfonyl chloride; at 50 ℃; for 18h;
DOI:10.3987/COM-89-5149

Reference yield:

: 485-47-2
indan-1,2,3-trione hydrate

: 128404-62-6
13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetic acid / 4 h / Heating

2: 84 percent / tosyl chloride / 18 h / 50 °C

With p-toluenesulfonyl chloride; In acetic acid;
DOI:10.3987/COM-89-5149

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 128404-62-6
13-<3'-nitrobenzoyl>indeno<2,1-b>benzoindolizin-12-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetic acid / 4 h / Heating

2: 84 percent / tosyl chloride / 18 h / 50 °C

With p-toluenesulfonyl chloride; In acetic acid;
DOI:10.3987/COM-89-5149