3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole

Base Information

• Chemical Name: 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole
• CAS No.: 96965-00-3
• Molecular Formula: C₁₉H₁₇Cl₂NO₃S
• Molecular Weight: 410.321

Synonyms:3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole

Chemical Property of 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole

Chemical Property:

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Technology Process of 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole

There total 3 articles about 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-(phenylsulfonyl)propyne (2525-41-9) + 3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide (13456-86-5) → 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole (96965-00-3)

Guidance literature:

In benzene; for 24h; Heating;

Reference yield: 57.0%

1-phenylsulfonyl-2-propanone (5000-44-2) + 3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide (13456-86-5) → 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole (96965-00-3)

Guidance literature:

With sodium hydroxide; In ethanol; for 0.5h; Heating;

DOI:10.1021/jo00217a037

Reference yield: 21.0%

phenylsulfonylpropa-1,2-diene (2525-42-0) + 3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide (13456-86-5) → 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-methyl-4-(phenylsulfonyl)isoxazole (96965-00-3) + 3-(3,5-dichloro-2,4,6-trimethylphenyl)-4-<(phenylsulfonyl)methyl>isoxazole (96965-04-7) + 3-(3,5-dichloro-2,4,6-trimethylphenyl)-5-<(phenylsulfonyl)methyl>isoxazole (96965-01-4) + 3,3'-bis(3,5-dichloro-2,4,6-trimethylphenyl)-5-(phenylsulfonyl)-4,5'-spirobi(2-isoxazoline) (96965-02-5)

Guidance literature:

In tetrachloromethane; for 9h; Further byproducts given; Heating;

DOI:10.1021/jo00217a037

upstream raw materials:

1-(phenylsulfonyl)propyne

3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide

1-phenylsulfonyl-2-propanone

phenylsulfonylpropa-1,2-diene

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