1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

Base Information

Chemical Name:1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea
CAS No.:181960-86-1
Molecular Formula:C₄₁H₄₈N₂O₁₀S
Molecular Weight:760.906
Hs Code.:

1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

Synonyms:1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

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Chemical Property of 1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

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Technology Process of 1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

There total 6 articles about 1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 181960-85-0
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thioureido]-tetrahydro-pyran-3-yl ester

: 181960-86-1
1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

Guidance literature:: With potassium hydroxide; In ethanol; at 25 ℃; for 0.5h;
DOI:10.1016/0008-6215(96)00090-0

Reference yield:

: 13992-25-1
1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

: 181960-86-1
1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / hydrogen / Pd(OH)2-on-charcoal / tetrahydrofuran; ethanol; H₂O / 3 h / 24 °C

2: 217 mg / tetrahydrofuran / 48 h / 25 °C

3: 84 percent / KOH / aq. ethanol / 0.5 h / 25 °C

With potassium hydroxide; hydrogen; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; water;
DOI:10.1016/0008-6215(96)00090-0

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 181960-86-1
1-((2R,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-thiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaN₃ / acetonitrile / 12 h / Heating

2: 69 percent / hydrogen / Pd(OH)2-on-charcoal / tetrahydrofuran; ethanol; H₂O / 3 h / 24 °C

3: 217 mg / tetrahydrofuran / 48 h / 25 °C

4: 84 percent / KOH / aq. ethanol / 0.5 h / 25 °C

With potassium hydroxide; sodium azide; hydrogen; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; water; acetonitrile;
DOI:10.1016/0008-6215(96)00090-0