allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Base Information

Chemical Name:allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside
CAS No.:230966-77-5
Molecular Formula:C₄₇H₇₄Cl₃NO₁₀
Molecular Weight:919.464
Hs Code.:

Synonyms:allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

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Chemical Property of allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

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Technology Process of allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

There total 5 articles about allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 87357-76-4
(R)-3-(dodecanoyloxy)tetradecanoic acid

: 183388-21-8
allyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 230966-77-5
allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/S0040-4020(02)01067-0

Reference yield:

: 112-54-9
Dodecanal

: 230966-77-5
allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: (-)-diisopinocamphenylborane chloride / diethyl ether / -78 °C

2: pyridine

3: potassium permanganate; acetic acid / hexane

4: dmap; dicyclohexyl-carbodiimide / dichloromethane

With pyridine; dmap; potassium permanganate; acetic acid; dicyclohexyl-carbodiimide; (-)-diisopinocamphenylborane chloride; In diethyl ether; hexane; dichloromethane;

Reference yield:

: 125946-60-3
(4R)-tetradecanoyloxy-1-pentadcene

: 230966-77-5
allyl (R)-4,6-O-benzylidene-2-deoxy-3-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: potassium permanganate; acetic acid / hexane

2: dmap; dicyclohexyl-carbodiimide / dichloromethane

With dmap; potassium permanganate; acetic acid; dicyclohexyl-carbodiimide; In hexane; dichloromethane;