ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

Base Information

Chemical Name:ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate
CAS No.:1369958-18-8
Molecular Formula:C₂₇H₂₉NO₆S
Molecular Weight:495.596
Hs Code.:

Synonyms:ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

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Chemical Property of ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

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Technology Process of ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

There total 4 articles about ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1369958-18-8
ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 5 h / 20 °C / Cooling with ice; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / chloroform / 1 h / 20 °C / Cooling with ice

3: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

4: tin(ll) chloride / ethyl acetate / 2 h / 80 °C

5: pyridine / Dichlorodifluoromethane / 0 °C / Inert atmosphere

With pyridine; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; tin(ll) chloride; In dichloromethane; chloroform; Dichlorodifluoromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1369958-15-5
ethyl 4-(benzyloxy)-2-[(4-nitrophenyl)sulfonyl]butanoate

: 1369958-18-8
ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tin(ll) chloride / ethyl acetate / 2 h / 80 °C

2: pyridine / Dichlorodifluoromethane / 0 °C / Inert atmosphere

With pyridine; tin(ll) chloride; In Dichlorodifluoromethane; ethyl acetate;

Reference yield:

: 75032-27-8
ethyl <(p-nitrophenyl)thio>acetate

: 1369958-18-8
ethyl 4-(benzyloxy)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfonyl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1 h / 20 °C / Cooling with ice

2: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

3: tin(ll) chloride / ethyl acetate / 2 h / 80 °C

4: pyridine / Dichlorodifluoromethane / 0 °C / Inert atmosphere

With pyridine; tetra-(n-butyl)ammonium iodide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; tin(ll) chloride; In chloroform; Dichlorodifluoromethane; ethyl acetate; N,N-dimethyl-formamide;