((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt

Base Information

Chemical Name:((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt
CAS No.:184642-96-4
Molecular Formula:C₃₂H₃₅CoO
Molecular Weight:494.622
Hs Code.:

Synonyms:((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt

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Chemical Property of ((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt

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Technology Process of ((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt

There total 1 articles about ((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: ((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(methoxycarbonyl)cyclopentadienyl)cobalt

: 591-51-5
phenyllithium

: 184642-96-4
((1,2,8,9-η)-tricyclo[7.5.0.0(1.7)]tetradeca-1,8-diene)(η(5)-(diphenylhydroxymethyl)cyclopentadienyl)cobalt

Guidance literature:: With H₂O; In tetrahydrofuran; hexane; -78°C (60 min), H2O addn.; extg. (ether), wasshing (NaHCO3 satd. soln.), drying (MgSO4), concg. (vac.), chromy. (alumina, 6% H2O / 1 : 20 ether / n-pentane); elem. anal.;
DOI:10.1021/om960694d