1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester

Base Information

• Chemical Name: 1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester
• CAS No.: 1071851-10-9
• Molecular Formula: C₅₅H₉₀N₂O₈Si₃
• Molecular Weight: 991.585

Synonyms:1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester

Chemical Property of 1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester

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Technology Process of 1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester

There total 1 articles about 1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1⁽²³⁾,6,8,10,16,20⁽²⁴⁾,21-heptaen-13-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

C57H94N2O8Si3 (1071850-89-9) → 1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1(23),6,8,10,16,20(24),21-heptaen-13-yl ester (1071851-10-9)

Guidance literature:

With Grubbs catalyst first generation; In dichloromethane; at 23 ℃; for 71h; Inert atmosphere; Darkness;

DOI:10.1002/anie.200802079

Reference yield: 95.0%

1-[(cyclohex-1-enecarbonyl)-amino]-cyclopropanecarboxylic acid (5R,6E,8E,10E,13S,14S,15R,16Z)-5-methoxy-14,16-dimethyl-3-oxo-15,22,24-tris(triethylsiloxy)-2-aza-bicyclo[18.3.1]tetracosa-1(23),6,8,10,16,20(24),21-heptaen-13-yl ester (1071851-10-9) → (+)-cytotrienin A (189010-85-3)

Guidance literature:

With Amberlyst 15; water; In tetrahydrofuran; at 23 ℃; for 47h; Inert atmosphere; Darkness;

DOI:10.1002/anie.200802079

upstream raw materials:

C₅₇H₉₄N₂O₈Si₃

Downstream raw materials:

(+)-cytotrienin A

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