(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

Base Information

Chemical Name:(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester
CAS No.:1027197-11-0
Molecular Formula:C₁₉H₃₀O₆S
Molecular Weight:386.51
Hs Code.:

Synonyms:(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

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Chemical Property of (3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

Chemical Property:

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Technology Process of (3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

There total 4 articles about (3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 75-24-1
trimethylaluminum

: 154867-97-7
(2E,4S)-methyl 4-(methoxymethoxy)-2-(phenylsulfonyl)-2-nonenoate

: 1027197-11-0
(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

Guidance literature:: In dichloromethane; at -20 ℃; for 2h;
DOI:10.1016/S0040-4020(01)80181-2

Reference yield:

: 140174-83-0
(E)-(S)-1-Benzenesulfonyl-oct-1-en-3-ol

: 1027197-11-0
(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus pentoxide / CHCl₃ / 1.5 h / Ambient temperature

2: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C

3: 89 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

4: 88 percent / CH₂Cl₂ / 2 h / -20 °C

With phosphorus pentaoxide; n-butyllithium; sodium hydrogencarbonate; In tetrahydrofuran; hexane; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80181-2

Reference yield:

: ((E)-(S)-3-Methoxymethoxy-oct-1-ene-1-sulfonyl)-benzene

: 1027197-11-0
(3R,4S)-2-Benzenesulfonyl-4-methoxymethoxy-3-methyl-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C

2: 89 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

3: 88 percent / CH₂Cl₂ / 2 h / -20 °C

With n-butyllithium; sodium hydrogencarbonate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80181-2