C₁₇H₂₄O₆

Base Information

• Chemical Name: C₁₇H₂₄O₆
• CAS No.: 934747-56-5
• Molecular Formula: C₁₇H₂₄O₆
• Molecular Weight: 324.374
• Mol file: 934747-56-5.mol

Synonyms:C₁₇H₂₄O₆

Chemical Property of C₁₇H₂₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₄O₆

There total 1 articles about C₁₇H₂₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C18H22O7 (934747-55-4) → C17H24O6 (934747-56-5)

Guidance literature:

With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; ethanol; at -78 ℃;

DOI:10.1016/j.tetlet.2007.01.102

Reference yield:

C17H24O6 (934747-56-5) → C34H46O4SSi (934747-66-7)

Guidance literature:

Multi-step reaction with 12 steps

1.1: n-Bu₃P / tetrahydrofuran / 20 °C

2.1: H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

3.1: dimethylformamide; tetrahydrofuran / 0 °C

4.1: 96 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 20 °C

5.1: TFA / tetrahydrofuran / 20 °C

5.2: 98 percent / imidazole / dimethylformamide / 20 °C

6.1: m-CPBA; NaHCO₃ / CH₂Cl₂ / 0 - 20 °C

7.1: LiAlH₄ / diethyl ether / -20 °C

8.1: TBAI; NaH / tetrahydrofuran; dimethylformamide / 20 °C

8.2: 51 percent / CSA / methanol; tetrahydrofuran / 0 °C

9.1: 95 percent / iodine; PPh₃; imidazole / tetrahydrofuran / 20 °C

10.1: 90 percent / dimethylsulfoxide / 45 °C

11.1: DIBAL-H / CH₂Cl₂ / -95 °C

11.2: 83 percent / NaBH₄ / CH₂Cl₂; methanol / -20 - 20 °C

12.1: 95 percent / nBu₃P; pyridine / 20 °C

With pyridine; 1H-imidazole; lithium aluminium tetrahydride; tributylphosphine; dihydrogen peroxide; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2007.01.102

Reference yield:

C17H24O6 (934747-56-5) → C47H60O10Si

Guidance literature:

Multi-step reaction with 20 steps

1.1: n-Bu₃P / tetrahydrofuran / 20 °C

2.1: H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

3.1: dimethylformamide; tetrahydrofuran / 0 °C

4.1: 96 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 20 °C

5.1: TFA / tetrahydrofuran / 20 °C

5.2: 98 percent / imidazole / dimethylformamide / 20 °C

6.1: m-CPBA; NaHCO₃ / CH₂Cl₂ / 0 - 20 °C

7.1: LiAlH₄ / diethyl ether / -20 °C

8.1: TBAI; NaH / tetrahydrofuran; dimethylformamide / 20 °C

8.2: 51 percent / CSA / methanol; tetrahydrofuran / 0 °C

9.1: 95 percent / iodine; PPh₃; imidazole / tetrahydrofuran / 20 °C

10.1: 90 percent / dimethylsulfoxide / 45 °C

11.1: DIBAL-H / CH₂Cl₂ / -95 °C

11.2: 83 percent / NaBH₄ / CH₂Cl₂; methanol / -20 - 20 °C

12.1: 95 percent / nBu₃P; pyridine / 20 °C

13.1: NCS / CH₂Cl₂; CCl₄ / 20 °C

14.1: 70 percent / AgOTf; 2,6-di-tert-butyl-4-methylpyridine; 4 Angstroem MS / CH₂Cl₂; CCl₄ / -90 - -15 °C

15.1: 93 percent / AgOTf; i-Pr₂NEt; 4 Angstroem MS / benzene / 20 °C

16.1: LiOH*H₂O / dioxane; H₂O / 20 °C

17.1: n-Bu₃P / dimethylformamide / 20 °C

18.1: 63 percent / n-Bu₃GeH; Et₃B / benzene

19.1: 52 percent / LiN(TMS)2 / tetrahydrofuran / -95 °C

20.1: 83 percent / Pd(OAc)2 / acetonitrile / 20 °C

With pyridine; 1H-imidazole; lithium hydroxide; N-chloro-succinimide; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; triethyl borane; tributylphosphine; 4 Angstroem MS; dihydrogen peroxide; iodine; silver trifluoromethanesulfonate; tributylgermanium hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; lithium hexamethyldisilazane; palladium diacetate; Grubbs catalyst first generation; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; benzene; 20.1: Saegusa oxidation;

DOI:10.1016/j.tetlet.2007.01.102

upstream raw materials:

C₁₈H₂₂O₇

Downstream raw materials:

C₂₀H₂₆O₅

C₁₈H₂₂O₅

C₃₄H₄₆O₄SSi

C₃₄H₄₅ClO₄SSi