(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

Base Information

Chemical Name:(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene
CAS No.:120476-89-3
Molecular Formula:C₁₈H₃₃NO₄
Molecular Weight:327.464
Hs Code.:

Synonyms:(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

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Technology Process of (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

There total 4 articles about (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 107-30-2
chloromethyl methyl ether

: 104856-06-6
tert-butyl [(1S,2S)-1-(cyclohexylmethyl)-2-hydroxy-3-butenyl]carbamate

: 120476-89-3
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; 1) 0 deg C, 15 min, 2) r.t., 14 h;
DOI:10.1021/jm00126a038

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 120476-89-3
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 83 percent / diisopropylethylamine / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) r.t., 14 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm00126a038

Reference yield:

: 104856-09-9
(3S,4S)-4-amino-5-cyclohexyl-3-hydroxy-1-pentene

: 120476-89-3
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-3-(methoxymethoxy)-1-pentene

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 83 percent / diisopropylethylamine / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) r.t., 14 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm00126a038