2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine

Base Information

• Chemical Name: 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine
• CAS No.: 274696-26-3
• Molecular Formula: C₁₈H₁₉N₂OP
• Molecular Weight: 310.335
• Mol file: 274696-26-3.mol

Synonyms:2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine

Chemical Property of 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine

There total 1 articles about 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ³-phospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(4,5-dihydro-3-furyl)phosphonous dichloride (66517-43-9) + N,N'-diphenylethylenediamine (150-61-8) → 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ3-phospholidine (274696-26-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1007/BF02499078

Reference yield: 80.0%

2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ3-phospholidine (274696-26-3) + N-phenyl-p-nitrobenzhydrazonoyl chloride (20147-55-1) → 5-(2-chloroethyl)-4-(N,N'-diphenylethylenediamino)-3-(p-nitrophenyl)-1-phenyl-1,4-dihydro-1,2,4λ5-diazaphosphorine

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1007/s11172-006-0016-6

Reference yield: 72.0%

ethoxycarbonylformyl chloride p-bromophenylhydrazone (27143-10-8) + 2-(4,5-dihydrofur-3-yl)-1,3-diphenyl-1,3-diaza-2λ3-phospholidine (274696-26-3) → 1-(p-bromophenyl)-5-(2-chloroethyl)-4-(N,N'-diphenylethylenediamino)-3-ethoxycarbonyl-1,4-dihydro-1,2,4λ5-diazaphosphorine

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1007/s11172-006-0016-6

upstream raw materials:

(4,5-dihydro-3-furyl)phosphonous dichloride

N,N'-diphenylethylenediamine