N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine

Base Information

• Chemical Name: N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine
• CAS No.: 1349752-26-6
• Molecular Formula: C₃₆H₄₈N₈O₈
• Molecular Weight: 720.826

Synonyms:N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine

Chemical Property of N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine

Chemical Property:

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Technology Process of N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine

There total 1 articles about N₂-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(E)-4-(dibenzylamino)-4-oxobut-2-enoic acid (863647-71-6) + Boc-Piz-Ala-Ala-NH-NH-CH2COOEt → N2-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N1-carbamoylmethyl-N1-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine (1349752-26-6)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at -10 - 20 ℃;

DOI:10.1021/jm900849h

Reference yield: 99.0%

N2-(4-(tert-butoxycarbonyl)piperazin-1-ylcarbonylalanylalanyl)-N1-carbamoylmethyl-N1-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine (1349752-26-6) → N2-(N-piperazinocarbonylalanylalanyl)-N1-carbamoylmethyl-N1-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine (1349490-65-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jm900849h

upstream raw materials:

(E)-4-(dibenzylamino)-4-oxobut-2-enoic acid

Downstream raw materials:

N₂-(N-piperazinocarbonylalanylalanyl)-N₁-carbamoylmethyl-N₁-trans-(3-dibenzylcarbamoylpropenoyl)hydrazine

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