C₃₃H₄₄O₇

Base Information

Chemical Name:C₃₃H₄₄O₇
CAS No.:1375412-61-5
Molecular Formula:C₃₃H₄₄O₇
Molecular Weight:552.708
Hs Code.:

C<sub>33</sub>H<sub>44</sub>O<sub>7</sub>

Synonyms:C₃₃H₄₄O₇

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Chemical Property of C₃₃H₄₄O₇

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Technology Process of C₃₃H₄₄O₇

There total 15 articles about C₃₃H₄₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1375412-60-4
C₃₉H₅₈O₇Si

: 1375412-61-5
C₃₃H₄₄O₇

Guidance literature:: With pyridine; hydrogen fluoride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-61-5
C₃₃H₄₄O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

6.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

7.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

8.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

9.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

10.1: Grela's catalyst; 2,3,5,6-tetrafluoro-1,4-benzoquinone / dichloromethane / 3 h / 60 °C / Inert atmosphere

10.2: 2 h / 20 °C

11.1: Jones reagent / acetone / 1 h / 0 °C

12.1: pyridine; hydrogen fluoride / tetrahydrofuran / 3 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; Jones reagent; n-butyllithium; samarium diiodide; triphenyl-arsane; 2,3,5,6-tetrafluoro-1,4-benzoquinone; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 2,4,6-trichlorobenzoyl chloride; Grela's catalyst; hydrogen fluoride; silver perchlorate; 3-chloro-benzenecarboperoxoic acid; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement / 7.1: Evans-Tishchenko reduction / 9.1: Stille coupling;
DOI:10.1002/anie.201108692

Reference yield:

: 37715-31-4
(E)-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-enyl acetate

: 1375412-61-5
C₃₃H₄₄O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

2.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

3.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

3.2: 0.5 h

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

4.2: 1 h / -50 - -45 °C

4.3: 2 h / -70 - 0 °C

5.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

6.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

7.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

8.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

9.1: Grela's catalyst; 2,3,5,6-tetrafluoro-1,4-benzoquinone / dichloromethane / 3 h / 60 °C / Inert atmosphere

9.2: 2 h / 20 °C

10.1: Jones reagent / acetone / 1 h / 0 °C

11.1: pyridine; hydrogen fluoride / tetrahydrofuran / 3 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; Jones reagent; n-butyllithium; samarium diiodide; triphenyl-arsane; 2,3,5,6-tetrafluoro-1,4-benzoquinone; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 2,4,6-trichlorobenzoyl chloride; Grela's catalyst; hydrogen fluoride; silver perchlorate; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; dimethyl sulfate; acetonitrile; 4.3: Brook rearrangement / 6.1: Evans-Tishchenko reduction / 8.1: Stille coupling;
DOI:10.1002/anie.201108692