Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

Base Information

Chemical Name:Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)
CAS No.:1312415-91-0
Molecular Formula:C₃₀H₄₁N₇O₁₀
Molecular Weight:659.696
Hs Code.:

Synonyms:Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

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Chemical Property of Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

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Technology Process of Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

There total 8 articles about Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312415-87-4
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz) ethyl ester

: 1312415-91-0
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.75h;
DOI:10.1021/jo200482d

Reference yield:

: 150438-69-0
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine

: 1312415-91-0
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / 1,2-dimethoxyethane / 0.5 h / 0 °C / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: propylamine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

4.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4.2: 24 h / 50 °C / Inert atmosphere

5.1: water; sodium hydroxide / tetrahydrofuran / 0.75 h / 0 °C

With 4-methyl-morpholine; propylamine; di-isopropyl azodicarboxylate; water; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; dicyclohexyl-carbodiimide; triphenylphosphine; sodium hydroxide; isobutyl chloroformate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; 2.1: Mitsunobu reaction;
DOI:10.1021/jo200482d

Reference yield:

: 1312415-84-1
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine-Ψ[CH2N(o,p-diNBS)]Gly-OEt

: 1312415-91-0
Boc-(2-(2-methoxyethoxy)ethyl)-L-serine adenine(Cbz)

Guidance literature:: Multi-step reaction with 3 steps

1.1: propylamine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

2.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

2.2: 24 h / 50 °C / Inert atmosphere

3.1: water; sodium hydroxide / tetrahydrofuran / 0.75 h / 0 °C

With propylamine; water; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200482d