9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine

Base Information

• Chemical Name: 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine
• CAS No.: 104532-10-7
• Molecular Formula: C₄₈H₄₁N₅O₄
• Molecular Weight: 751.885

Synonyms:9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine

Chemical Property of 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine

Chemical Property:

Purity/Quality:

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Technology Process of 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine

There total 10 articles about 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N²-triphenylmethylguanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N2,O5'-bis(triphenylmethyl)-3'-O-p-toluenesulfonyl-2',3'-secoguanosine (104548-77-8) → 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N2-triphenylmethylguanine (104532-10-7)

Guidance literature:

With sodium methylate; In methanol; at 60 ℃; for 20h;

DOI:10.1021/jm00162a005

Reference yield: 82.0%

N2,O5'-bis(triphenylmethyl)-2',3'-di-O-p-toluenesulfonyl-2',3'-secoguanosine (104532-09-4) → 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N2-triphenylmethylguanine (104532-10-7)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; at 60 ℃; for 20h;

DOI:10.1021/jm00162a005

Reference yield: 44.0%

N2,O5'-bis(triphenylmethyl)-2'-O-p-toluenesulfonyl-2',3'-secoguanosine (104548-76-7) → 9-<6(S)-<(triphenylmethoxy)methyl>-1,4-dioxacyclohexan-2(R)-yl>-N2-triphenylmethylguanine (104532-10-7) + N2,O5'-bis(triphenylmethyl)secoguanosine (104532-08-3)

Guidance literature:

With sodium methylate; at 60 ℃; for 20h;

DOI:10.1021/jm00162a005

upstream raw materials:

sodium methylate

N²,O^5'-bis(triphenylmethyl)-2',3'-di-O-p-toluenesulfonyl-2',3'-secoguanosine

N²,O^5'-bis(triphenylmethyl)-3'-O-p-toluenesulfonyl-2',3'-secoguanosine

N²,O^5'-bis(triphenylmethyl)-2'-O-p-toluenesulfonyl-2',3'-secoguanosine

Downstream raw materials:

9-<6(R)-(hydroxymethyl)-1,4-dioxacyclohexan-2(R)-yl>guanine

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