C₂₄H₂₅FN₆O₃

Base Information

Chemical Name:C₂₄H₂₅FN₆O₃
CAS No.:1431871-87-2
Molecular Formula:C₂₄H₂₅FN₆O₃
Molecular Weight:464.499
Hs Code.:

C<sub>24</sub>H<sub>25</sub>FN<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₅FN₆O₃

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Chemical Property of C₂₄H₂₅FN₆O₃

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Technology Process of C₂₄H₂₅FN₆O₃

There total 7 articles about C₂₄H₂₅FN₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431871-85-0
C₂₄H₂₅FN₆O₃

: 1431871-87-2
C₂₄H₂₅FN₆O₃

: 1431871-86-1
C₂₄H₂₅FN₆O₃

Guidance literature:: With CHIRALPAK AD-H column; In methanol; carbon dioxide; Resolution of racemate; liquid CO₂;

Reference yield:

: 1431872-97-7
C₇H₄BrN₃O

: 1431871-87-2
C₂₄H₂₅FN₆O₃

: 1431871-86-1
C₂₄H₂₅FN₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

3.1: hydrogenchloride / 1,4-dioxane / 100 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C / Inert atmosphere

4.2: 48 h / 20 °C

5.1: CHIRALPAK AD-H column / methanol; carbon dioxide / Resolution of racemate; liquid CO₂

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; trichlorophosphate; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; carbon dioxide; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1431872-96-6
C₈H₈ClN₃O₂

: 1431871-87-2
C₂₄H₂₅FN₆O₃

: 1431871-86-1
C₂₄H₂₅FN₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

4.1: hydrogenchloride / 1,4-dioxane / 100 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C / Inert atmosphere

5.2: 48 h / 20 °C

6.1: CHIRALPAK AD-H column / methanol; carbon dioxide / Resolution of racemate; liquid CO₂

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; sodium hydride; sodium carbonate; acetic acid; N,N-dimethyl-formamide; trichlorophosphate; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; carbon dioxide; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;