8-methoxy-9-tosyl-3,4-dihydro-β-carboline

Base Information

Chemical Name:8-methoxy-9-tosyl-3,4-dihydro-β-carboline
CAS No.:1421052-25-6
Molecular Formula:C₁₉H₁₈N₂O₃S
Molecular Weight:354.43
Hs Code.:

Synonyms:8-methoxy-9-tosyl-3,4-dihydro-β-carboline

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Chemical Property of 8-methoxy-9-tosyl-3,4-dihydro-β-carboline

Chemical Property:

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Technology Process of 8-methoxy-9-tosyl-3,4-dihydro-β-carboline

There total 3 articles about 8-methoxy-9-tosyl-3,4-dihydro-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-16-3
p-toluenesulfonyl fluoride

: 31652-37-6
CGS 19281A

: 1421052-25-6
8-methoxy-9-tosyl-3,4-dihydro-β-carboline

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja310718f

Reference yield:

: 3610-36-4
2-(6-methoxy-1H-indol-3-yl)ethanamine

: 1421052-25-6
8-methoxy-9-tosyl-3,4-dihydro-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 16 h / 100 °C / Inert atmosphere

2: trichlorophosphate / acetonitrile / 3 h / 0 °C / Inert atmosphere

3: caesium carbonate / N,N-dimethyl-formamide / 24 h / 23 °C / Inert atmosphere

With caesium carbonate; triethylamine; trichlorophosphate; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja310718f

Reference yield:

: 104509-98-0
N-(2-(6-methoxy-1H-indol-3-yl)ethyl)formamide

: 1421052-25-6
8-methoxy-9-tosyl-3,4-dihydro-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / acetonitrile / 3 h / 0 °C / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 24 h / 23 °C / Inert atmosphere

With caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja310718f