2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

Base Information

Chemical Name:2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid
CAS No.:1024035-87-7
Molecular Formula:C₂₂H₃₃N₃O₄
Molecular Weight:403.522
Hs Code.:

Synonyms:2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

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Chemical Property of 2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

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Technology Process of 2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

There total 5 articles about 2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₂₃H₃₅N₃O₄

: 1024035-87-7
2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

Guidance literature:: With sodium hydroxide; In methanol; at 25 ℃; for 32h;
DOI:10.1021/jm300592r

Reference yield:

: 1003872-51-2
2,6-dichloro-N-cyclohexyl-pyridine-3-carboxamide

: 1024035-87-7
2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 150 °C / Microwave irradiation

2: potassium carbonate / propyl cyanide / 4 h / 170 °C / Microwave irradiation

3: sodium hydroxide / methanol / 32 h / 25 °C

With sodium hexamethyldisilazane; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; propyl cyanide;
DOI:10.1021/jm300592r

Reference yield:

: 1024038-80-9
6-chloro-N-cyclohexyl-2-propoxynicotinamide

: 1024035-87-7
2-[(3S)-1-[5-(cyclohexylcarbamoyl)-6-propoxypyridin-2-yl]-3-piperidyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / propyl cyanide / 4 h / 170 °C / Microwave irradiation

2: sodium hydroxide / methanol / 32 h / 25 °C

With potassium carbonate; sodium hydroxide; In methanol; propyl cyanide;
DOI:10.1021/jm300592r