C₄₀H₇₀O₉Si₃

Base Information

Chemical Name:C₄₀H₇₀O₉Si₃
CAS No.:1579197-53-7
Molecular Formula:C₄₀H₇₀O₉Si₃
Molecular Weight:779.247
Hs Code.:

C<sub>40</sub>H<sub>70</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₄₀H₇₀O₉Si₃

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Chemical Property of C₄₀H₇₀O₉Si₃

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Technology Process of C₄₀H₇₀O₉Si₃

There total 7 articles about C₄₀H₇₀O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1579197-48-0
C₄₀H₇₂O₉Si₃

: 1579197-53-7
C₄₀H₇₀O₉Si₃

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 - 80 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja501460j

Reference yield:

: (E)-ethyl 3-(4-hydroxyphenyl)-2-methylacrylate

: 1579197-53-7
C₄₀H₇₀O₉Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: lithium hydroxide; water / methanol; tetrahydrofuran-d8 / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 - 63 °C / Inert atmosphere

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3 h / 20 - 60 °C / Inert atmosphere

4: potassium carbonate; water / 1 h / 20 °C

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 20 - 80 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; water; potassium carbonate; triphenylphosphine; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; tetrahydrofuran-d8; dimethyl sulfoxide; toluene;
DOI:10.1021/ja501460j

Reference yield:

: 113277-24-0,5325-37-1
(E)-3-(4-hydroxyphenyl)-2-methyl-prop-2-enoic acid

: 1579197-53-7
C₄₀H₇₀O₉Si₃

Guidance literature:: Multi-step reaction with 4 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 - 63 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3 h / 20 - 60 °C / Inert atmosphere

3: potassium carbonate; water / 1 h / 20 °C

4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 20 - 80 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; water; potassium carbonate; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; toluene;
DOI:10.1021/ja501460j