N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid

Base Information

• Chemical Name: N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid
• CAS No.: 130296-42-3
• Molecular Formula: C₃₉H₃₄N₂O₃
• Molecular Weight: 578.711

Synonyms:N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid

Chemical Property of N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid

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Technology Process of N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid

There total 5 articles about N²-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N2-(2,5-Di-tert-butylphenyl)-N1-ethyl-3,4:9,10-perylentetracarboxdiimid (130296-49-0) → N2-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid (130296-42-3)

Guidance literature:

With potassium hydroxide; In methanol; dimethyl sulfoxide; at 80 ℃; for 3h;

Reference yield:

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide (33955-42-9) → N2-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid (130296-42-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 40 percent / K₂CO₃ / dimethylformamide / 1) 16 h, 2) 80 deg C, 2 h

3: 68 percent / KOH / methanol; dimethylsulfoxide / 3 h / 80 °C

With potassium hydroxide; zinc diacetate; potassium carbonate; In quinoline; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

2,5-di-tert-butylaniline (21860-03-7) → N2-(2,5-Di-tert-butylphenyl)-N'-ethyl-3-amino-4,9,10-perylentricarbonsaeure-3,4-lactam-9,10-imid (130296-42-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 40 percent / K₂CO₃ / dimethylformamide / 1) 16 h, 2) 80 deg C, 2 h

3: 68 percent / KOH / methanol; dimethylsulfoxide / 3 h / 80 °C

With potassium hydroxide; zinc diacetate; potassium carbonate; In quinoline; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

upstream raw materials:

N²-(2,5-Di-tert-butylphenyl)-N¹-ethyl-3,4:9,10-perylentetracarboxdiimid

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide

2,5-di-tert-butylaniline

perylene-3,4,9,10-tetracarboxylic acid monoanhydride monopotassium carboxylate

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