6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

Base Information

Chemical Name:6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine
CAS No.:863591-95-1
Molecular Formula:C₂₉H₃₉N₅O₉SSi
Molecular Weight:661.808
Hs Code.:

Synonyms:6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

Chemical Property:

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Technology Process of 6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

There total 1 articles about 6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 115094-43-4
5'-O-(tert-butyldimethylsilyl)-2'-O-(p-tolylsulfonyl)adenosine

: Acetic acid (2R,3R,4R,5R)-5-(6-acetylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-4-(toluene-4-sulfonyloxy)-tetrahydro-furan-3-yl ester

: 863591-95-1
6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

Guidance literature:: With pyridine; Heating;
DOI:10.1021/jo051256w

Reference yield: 85.0%

: 863591-95-1
6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

: 115094-43-4
5'-O-(tert-butyldimethylsilyl)-2'-O-(p-tolylsulfonyl)adenosine

Guidance literature:: In methanol; at 105 ℃; for 1.5h;
DOI:10.1021/jo051256w

Reference yield:

: 863591-95-1
6-di-N,N-3'-O-triacetyl-5'-O-tert-butyldimethylsilyl-2'-O-tosyladenosine

: Acetic acid (2R,3R,4R,5R)-5-(6-acetylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-4-(toluene-4-sulfonyloxy)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / methanol / 1.5 h / 105 °C

2: pyridine / Heating

With pyridine; In methanol;
DOI:10.1021/jo051256w