C₅₃H₆₅N₉O₁₁

Base Information

Chemical Name:C₅₃H₆₅N₉O₁₁
CAS No.:1425940-95-9
Molecular Formula:C₅₃H₆₅N₉O₁₁
Molecular Weight:1004.15
Hs Code.:

C<sub>53</sub>H<sub>65</sub>N<sub>9</sub>O<sub>11</sub>

Synonyms:C₅₃H₆₅N₉O₁₁

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Chemical Property of C₅₃H₆₅N₉O₁₁

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Technology Process of C₅₃H₆₅N₉O₁₁

There total 13 articles about C₅₃H₆₅N₉O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425940-94-8
C₅₃H₆₇N₉O₁₂

: 1425940-95-9
C₅₃H₆₅N₉O₁₁

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/ol4002762

Reference yield:

: 1147719-74-1
methyl 2-methyl-2-(2-nitrobenzamido)propanoate

: 1425940-95-9
C₅₃H₆₅N₉O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 3102.97 Torr

2.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

2.2: 8 h / Inert atmosphere; Reflux

3.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

6.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 20 °C

8.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

9.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 20 °C

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762

Reference yield:

: 221539-54-4
N-(2-aminobenzoyl)-α-methylalanine methyl ester

: 1425940-95-9
C₅₃H₆₅N₉O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

1.2: 8 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

4.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 20 °C

With lithium hydroxide monohydrate; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762