5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP

Base Information

• Chemical Name: 5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP
• CAS No.: 885109-27-3
• Molecular Formula: C₄₇H₆₁N₈O₂₂P₃
• Molecular Weight: 1182.96

Synonyms:5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP

Chemical Property of 5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP

Chemical Property:

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Technology Process of 5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP

There total 2 articles about 5-(2-(6-(N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

Nα,Nω1,Nω2-tricarbobenzoxy-L-arginine N-succinimidyl ester (132160-73-7,200191-86-2) + 5-(2-(6-aminohexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate → 5-(2-(6-(Nα,Nω1,Nω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP (885109-27-3)

Guidance literature:

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1016/j.bmc.2005.11.030

Reference yield:

Nα,Nω1,Nω2-tricarbobenzoxy-L-arginine (20888-05-5) → 5-(2-(6-(Nα,Nω1,Nω2-tricarbobenzoxy-L-arginamido)hexylamino)-2-oxoethyl)-dUTP (885109-27-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N'-dicyclohexylcarbodiimide / dimethylformamide / 19 h / 0 - 20 °C

2: 59 percent / NaHCO₃ / dimethylformamide; H₂O / 3 h / 20 °C

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2005.11.030

upstream raw materials:

N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginine N-succinimidyl ester

N^α,N^ω1,N^ω2-tricarbobenzoxy-L-arginine

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