Pd(PCy3)2(η2-carbon disulfide)

Base Information

Chemical Name:Pd(PCy3)2(η2-carbon disulfide)
CAS No.:81191-61-9
Molecular Formula:C₃₇H₆₆P₂PdS₂
Molecular Weight:743.431
Hs Code.:

Synonyms:Pd(PCy3)2(η2-carbon disulfide)

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Chemical Property of Pd(PCy3)2(η2-carbon disulfide)

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Technology Process of Pd(PCy3)2(η2-carbon disulfide)

There total 1 articles about Pd(PCy3)2(η2-carbon disulfide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 33309-88-5
palladium⁽⁰⁾bis(tricyclohexylphosphine)

: 81191-61-9
Pd(PCy3)2(η2-carbon disulfide)

Guidance literature:: With CS₂; In hexane; the mixt. was stirred for 15 min.;; filtration; washed with hexane; elem. anal.;;
DOI:10.1016/0022-328X(84)85061-5

Reference yield: 90.0%

: 81191-61-9
Pd(PCy3)2(η2-carbon disulfide)

: 89071-14-7
Pd*P(C₆H₁₁)3*CS₂={Pd(P(C₆H₁₁)3)CS₂}

Guidance literature:: With carbon disulfide; In carbon disulfide; acetone; Pd(PCy3)2(CS2) was stirred in a 1:1 mixt. of acetone and CS2 at room temp.;; the ppt. was collected on a filter, washed with acetone, and dried at 50°C in vac.; elem. anal.;;

Reference yield: 75.0%

: 81191-61-9
(tricyclohexylphosphine)2(η2-CS2)palladium

: 2622-14-2
tricyclohexylphosphine

: (tricyclohexylphosphine)2(dithiocarbonato)palladium(II)*dichloromethane

: (tricyclohexylphosphine)2(dithiocarbonato)palladium(II)*dichloromethane

Guidance literature:: With O₂; In carbon disulfide; benzene; addn. of CS2 to a soln. of the Pd-compd. in benzene, O2 is bubbled through for 12 h, addn. of 0.5 mmol of the phosphine; most of the solvent is evapd., addn. of ether, the resulting ppt. is filtered off and washed twice with two portions of ether, recrystn. from CH2Cl2/ether; elem. anal.;