2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

Base Information

Chemical Name:2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol
CAS No.:137344-98-0
Molecular Formula:C₂₂H₂₅N₃O₅
Molecular Weight:411.458
Hs Code.:

Synonyms:2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

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Chemical Property of 2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

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Technology Process of 2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

There total 3 articles about 2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137344-96-8
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allonhydroximo-1,5-lactone

: 137344-98-0
2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NEt₃ / CH₂Cl₂ / 0.33 h

2: 64 percent / NH₃ / methanol / 3.75 h

With ammonia; triethylamine; In methanol; dichloromethane;
DOI:10.1002/hlca.19910740625

Reference yield:

: 29873-94-7,137432-77-0,137432-78-1
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranose

: 137344-98-0
2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaOMe, NH₂OH*HCl / methanol / 4 h / 50 °C

2: 95 percent / NaIO₄, NaOAc / H₂O; ethanol / 18 h / 50 °C

3: 81 percent / NEt₃ / CH₂Cl₂ / 0.33 h

4: 64 percent / NH₃ / methanol / 3.75 h

With sodium periodate; hydroxylamine hydrochloride; ammonia; sodium methylate; sodium acetate; triethylamine; In methanol; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19910740625

Reference yield:

: 137344-94-6,137344-95-7
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allose oxime

: 137344-98-0
2-Acetamido-1,5-anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-hydrazi-D-allitol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaIO₄, NaOAc / H₂O; ethanol / 18 h / 50 °C

2: 81 percent / NEt₃ / CH₂Cl₂ / 0.33 h

3: 64 percent / NH₃ / methanol / 3.75 h

With sodium periodate; ammonia; sodium acetate; triethylamine; In methanol; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19910740625