C₁₄H₉Cl₂NS

Base Information

Chemical Name:C₁₄H₉Cl₂NS
CAS No.:1221931-88-9
Molecular Formula:C₁₄H₉Cl₂NS
Molecular Weight:294.204
Hs Code.:

C<sub>14</sub>H<sub>9</sub>Cl<sub>2</sub>NS

Synonyms:C₁₄H₉Cl₂NS

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Chemical Property of C₁₄H₉Cl₂NS

Chemical Property:

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Technology Process of C₁₄H₉Cl₂NS

There total 5 articles about C₁₄H₉Cl₂NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1221931-86-7
C₁₄H₁₁ClN₂S

: 1221931-88-9
C₁₄H₉Cl₂NS

Guidance literature:: With copper dichloride; isopentyl nitrite; In acetonitrile; at 50 ℃; for 2.33333h; Inert atmosphere; Cooling in ice;

Reference yield:

: 13382-43-9
2-methyl-5-aminobenzothiazole

: 1221931-88-9
C₁₄H₉Cl₂NS

Guidance literature:: Multi-step reaction with 4 steps

1: N-chloro-succinimide / isopropyl alcohol / 1.5 h / 20 °C

2: N-Bromosuccinimide / isopropyl alcohol / 0.25 h / 65 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 0.33 h / 140 °C / Inert atmosphere; Microwave irradiation

4: copper dichloride; isopentyl nitrite / acetonitrile / 2.33 h / 50 °C / Inert atmosphere; Cooling in ice

With N-chloro-succinimide; N-Bromosuccinimide; sodium carbonate; copper dichloride; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; isopropyl alcohol; acetonitrile;

Reference yield:

: 686747-15-9
4-chloro-2-methyl-benzothiazol-5-ylamine

: 1221931-88-9
C₁₄H₉Cl₂NS

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / isopropyl alcohol / 0.25 h / 65 °C / Inert atmosphere

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 0.33 h / 140 °C / Inert atmosphere; Microwave irradiation

3: copper dichloride; isopentyl nitrite / acetonitrile / 2.33 h / 50 °C / Inert atmosphere; Cooling in ice

With N-Bromosuccinimide; sodium carbonate; copper dichloride; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; isopropyl alcohol; acetonitrile;