2-bromo-2-4-dimethoxypropiophenone

Base Information

• Chemical Name: 2-bromo-2-4-dimethoxypropiophenone
• CAS No.: 117844-88-9
• Molecular Formula: C11H13 Br O3
• Molecular Weight: 273.12
• Mol file: 117844-88-9.mol

Synonyms:2-Bromo-1-(2,4-dimethoxyphenyl)propan-1-one

Chemical Property of 2-bromo-2-4-dimethoxypropiophenone

Chemical Property:

• PSA: 35.53000
• LogP: 2.66990

Purity/Quality:

98%min ^*data from raw suppliers

2-Bromo-1-(2,4-dimethoxyphenyl)propan-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromo-2-4-dimethoxypropiophenone

There total 1 articles about 2-bromo-2-4-dimethoxypropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4-dimethoxypropiophenone (831-00-5) → 2-Bromo-1-(2,4-dimethoxy-phenyl)-propan-1-one (117844-88-9)

Guidance literature:

With bromine; In tetrachloromethane; at 30 - 35 ℃;

Reference yield: 80.0%

2-Bromo-1-(2,4-dimethoxy-phenyl)-propan-1-one (117844-88-9) + thiourea (17356-08-0) → 4-(2,4-dimethoxyphenyl)-5-methyl-1,3-thiazol-2-amine (117844-98-1)

Guidance literature:

In ethanol; Heating;

Reference yield: 75.0%

ammonium dithiocarbamate (513-74-6) + 2-Bromo-1-(2,4-dimethoxy-phenyl)-propan-1-one (117844-88-9) → 4-(2,4-Dimethoxy-phenyl)-5-methyl-thiazole-2-thiol (117845-04-2)

Guidance literature:

In ethanol; Heating;

upstream raw materials:

2,4-dimethoxypropiophenone

Downstream raw materials:

4-(2,4-Dimethoxy-phenyl)-5-methyl-thiazole-2-thiol

4-(2,4-dimethoxyphenyl)-5-methyl-1,3-thiazol-2-amine

4-(2,4-Dimethoxy-phenyl)-5-methyl-2-methylsulfanyl-thiazole

N-[4-(2,4-Dimethoxy-phenyl)-5-methyl-thiazol-2-yl]-acetamide

Refernces