5-piperidylboronic acid

Base Information

Chemical Name:5-piperidylboronic acid
CAS No.:120347-74-2
Molecular Formula:C₅H₁₂BNO₂
Molecular Weight:128.967
Hs Code.:

Synonyms:5-piperidylboronic acid

Suppliers and Price of 5-piperidylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 5-piperidylboronic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-piperidylboronic acid

There total 1 articles about 5-piperidylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6612-51-7
1-trimethylsilanyl-1,2,3,6-tetrahydro-pyridine

: 120347-74-2
5-piperidylboronic acid

: 120347-72-0
C₅H₉NHB(OH)2

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; mixing of compd. (0°C, Ar atmosphere), stirring of mixt. (1h, room temp.), evapn., addn. of cold CH3OH, stirring under reflux (30 min), evapn., dissolving (HCl), refluxing (1h), evapn. (vac., 60°C, percolating ion exchange resin; evapn.;

Reference yield:

: 120347-74-2
5-piperidylboronic acid

: 6627-53-8
1-chloro-3-methoxy-4-nitrobenzene

: 1383682-75-4
C₁₂H₁₆N₂O₃

Guidance literature:: 5-piperidylboronic acid; 1-chloro-3-methoxy-4-nitrobenzene; With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 80 ℃; for 16h; Inert atmosphere;

With sodium carbonate; palladium; In 1,4-dioxane; at 85 ℃; for 4h;

Reference yield:

: 120347-74-2
5-piperidylboronic acid

: 1260868-83-4
C₁₂H₁₈N₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

1.2: 4 h / 85 °C

2.1: hydrogen; acetic acid / platinum(IV) oxide / 48 h / 20 °C / 6750.68 Torr

With hydrogen; sodium carbonate; acetic acid; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane;