4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Base Information

• Chemical Name: 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol
• CAS No.: 1026418-11-0
• Molecular Formula: C₂₄H₃₂N₂O₂S
• Molecular Weight: 412.596

Synonyms:4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Chemical Property of 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Chemical Property:

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Technology Process of 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

There total 3 articles about 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-(3,5-di-tert-butyl-4-hydroxy-phenyl)-ethanone (1027506-52-0) → 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol (1026418-11-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; chloroform; at 20 ℃; for 0.5h;

DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

(1H-benzimidazol-2-yl)methanethiol (4344-85-8) → 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol (1026418-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 2 h / 20 °C

2: NaBH₄ / CHCl₃; methanol / 0.5 h / 20 °C

With sodium tetrahydroborate; sodium hydride; In methanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

1,2-diamino-benzene (95-54-5) → 4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol (1026418-11-0)

Guidance literature:

Multi-step reaction with 3 steps

1: HCl / 5 h / Heating

2: NaH / dimethylformamide / 2 h / 20 °C

3: NaBH₄ / CHCl₃; methanol / 0.5 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium hydride; In methanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1016/S0223-5234(03)00144-2

upstream raw materials:

2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-(3,5-di-tert-butyl-4-hydroxy-phenyl)-ethanone

(1H-benzimidazol-2-yl)methanethiol

1,2-diamino-benzene

Downstream raw materials:

4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

2,6-di-tert-butyl-4-[2-(1-methanesulfonyl-1H-benzoimidazol-2-ylmethanesulfonyl)-vinyl]-phenol

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