Technology Process of C57H88N12O11
There total 8 articles about C57H88N12O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H26N2O5;
With
3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide;
In
N,N-dimethyl-formamide;
for 4h;
Automated synthesizer;
solid phase reaction;
With
piperidine;
In
N,N-dimethyl-formamide;
Automated synthesizer;
solid phase reaction;
C23H26N2O5; C26H32N2O5; C29H30N2O5; C40H47N3O8;
Further stages;
DOI:10.1016/j.bmcl.2011.01.005
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium cyanoborohydride; acetic acid / methanol / 0 - 20 °C
2.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide
3.1: 20 °C
4.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 4 h / Automated synthesizer; solid phase reaction
4.2: Automated synthesizer; solid phase reaction
With
sodium cyanoborohydride; acetic acid; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide
2.1: 20 °C
3.1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 4 h / Automated synthesizer; solid phase reaction
3.2: Automated synthesizer; solid phase reaction
With
3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.005
