2-Bromoundec-1-ene

Base Information

• Chemical Name: 2-Bromoundec-1-ene
• CAS No.: 145732-28-1
• Molecular Formula: C₁₁H₂₁Br
• Molecular Weight: 233.192
• DSSTox Substance ID: DTXSID80373769
• Nikkaji Number: J806.301J
• Wikidata: Q82162101
• Mol file: 145732-28-1.mol

Synonyms:2-bromoundec-1-ene;2-BROMO-1-UNDECENE;145732-28-1;1-Undecene, 2-bromo-;MFCD00671863;DTXSID80373769;AKOS016016642

Chemical Property of 2-Bromoundec-1-ene

Chemical Property:

• Vapor Pressure: 0.0447mmHg at 25°C
• XLogP3: 6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 8
• Exact Mass: 232.08266
• Heavy Atom Count: 12
• Complexity: 108

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-1-undecene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCC(=C)Br

Technology Process of 2-Bromoundec-1-ene

There total 3 articles about 2-Bromoundec-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1-Iodooctane (629-27-6) + (2-bromoallyl)(phenyl)sulfane (139930-06-6) → 2-Bromo-undec-1-ene (145732-28-1)

Guidance literature:

With bis(tri-n-butyltin); In benzene; for 3h; Irradiation;

DOI:10.1016/S0040-4039(00)60898-5

Reference yield: 36.0%

1-bromo-octane (111-83-1) + (2-bromoallyl)(phenyl)sulfane (139930-06-6) → 2-Bromo-undec-1-ene (145732-28-1)

Guidance literature:

With bis(tri-n-butyltin); In benzene; for 12h; Irradiation;

DOI:10.1016/S0040-4039(00)60898-5

Reference yield:

2-bromoallyl bromide (513-31-5) → 2-Bromo-undec-1-ene (145732-28-1)

Guidance literature:

In tetrahydrofuran; for 13h; Ambient temperature;

DOI:10.1055/s-1987-28164

upstream raw materials:

1-Iodooctane

(2-bromoallyl)(phenyl)sulfane

1-bromo-octane

2-bromoallyl bromide

Downstream raw materials:

2-methyl-undec-1-ene

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