acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

Base Information

Chemical Name:acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique
CAS No.:74444-87-4
Molecular Formula:C₁₃H₁₃ClO₄
Molecular Weight:268.697
Hs Code.:

Synonyms:acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

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Chemical Property of acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

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Technology Process of acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

There total 3 articles about acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 74444-84-1
Potassium; 2-(4-chloro-phenyl)-1-ethoxycarbonyl-cyclopropanecarboxylate

: 74444-87-4
acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

Guidance literature:: With hydrogenchloride; In water;

Reference yield: 86.0%

: 74444-83-0
2-(4-chlorophenyl)cyclopropane-1,1-dicarboxylic acid diethyl ester

: 74444-87-4
acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

Guidance literature:: 2-(4-chlorophenyl)cyclopropane-1,1-dicarboxylic acid diethyl ester; With water; sodium hydroxide; In ethanol; at 20 ℃; for 12h;

With potassium hydrogensulfate; In water;
DOI:10.1016/j.ejmech.2010.05.034

Reference yield:

: 6827-40-3
diethyl 4-chlorobenzylidenemalonate

: 74444-87-4
acide parachlorophenyl-2 ethoxycarbonyl-1 cyclopropane carboxylique

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaOH / 1.) hexane, DMSO, 1h, rt; 2.) 1h, 50 deg C

2: 80 percent / aq. KOH / ethanol; methanol / 1 h / Heating

3: 94 percent / 2N HCl / H₂O

With hydrogenchloride; potassium hydroxide; sodium hydroxide; In methanol; ethanol; water;