(Z)-2-ethylidene cyclohexanone

Base Information

• Chemical Name: (Z)-2-ethylidene cyclohexanone
• CAS No.: 7417-54-1
• Molecular Formula: C₈H₁₂O
• Molecular Weight: 124.183
• Mol file: 7417-54-1.mol

Synonyms:(Z)-2-ethylidene cyclohexanone

Chemical Property of (Z)-2-ethylidene cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-2-ethylidene cyclohexanone

There total 2 articles about (Z)-2-ethylidene cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → (Z)-2-ethylidene cyclohexanone (7417-54-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Na, EtOH / 1.) 0 deg C, 2.) 0 deg C, 45 min

2: oxalic acid dihydrate / cyclohexanone

With ethanol; sodium; oxalic acid; In cyclohexanone;

DOI:10.1021/jo00142a018

Reference yield:

→ (Z)-2-ethylidene cyclohexanone (7417-54-1)

Guidance literature:

2-(1-Hydroxy-ethyl)-cyclohexanon, Dehydratation m. Saeure, in geringer Menge neben d. trans-Isomeren;

Reference yield: 77.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + (Z)-2-ethylidene cyclohexanone (7417-54-1) → 1-<1-(6-Oxo-1-cyclohexenyl)ethyl>-4-phenyl-1,2,4-triazolidine-3,5-dione (74542-34-0)

Guidance literature:

In dichloromethane; Ambient temperature;

DOI:10.1021/jo01310a007

upstream raw materials:

cyclohexanone

Downstream raw materials:

1-Ethinyl-2-ethyliden-cyclohexan-1-ol

1-<1-(6-Oxo-1-cyclohexenyl)ethyl>-4-phenyl-1,2,4-triazolidine-3,5-dione

2-[(2E,4E)-5-Dimethylamino-penta-2,4-dien-(E)-ylidene]-6-[(E)-3-dimethylamino-prop-2-en-(E)-ylidene]-cyclohexanone

2-[(E)-3-Dimethylamino-prop-2-en-(E)-ylidene]-6-eth-(E)-ylidene-cyclohexanone