N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

Base Information

Chemical Name:N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester
CAS No.:1378235-85-8
Molecular Formula:C₄₅H₅₇N₇O₉
Molecular Weight:839.989
Hs Code.:

N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

Synonyms:N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

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Chemical Property of N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

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Technology Process of N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

There total 4 articles about N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 34619-03-9
tert-butyldicarbonate

: 1378235-84-7
(3-benzyloxycarbonylamino-propyl)-[4-(benzyloxycarbonyl-{3-[(6-hydrazino-pyridine-3-carbonyl)-amino]-propyl}-amino)-butyl]-carbamic acid benzyl ester

: 1378235-85-8
N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 5326-23-8
6-Chloro-3-pyridinecarboxylic acid

: 1378235-85-8
N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / acetonitrile / 1.5 h / 20 °C

2: hydrazine hydrate / 2 h / Reflux

3: triethylamine / tetrahydrofuran / 2 h / 20 °C

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; hydrazine hydrate; triethylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 1378235-83-6
(3-benzyloxycarbonylamino-propyl)-[4-(benzyloxycarbonyl-{3-[(6-chloro-pyridine-3-carbonyl)-amino]-propyl}-amino)-butyl]-carbamic acid benzyl ester

: 1378235-85-8
N'-{5-[3-(benzyloxycarbonyl-{4-[benzyloxycarbonyl-(3-benzyloxycarbonylamino-propyl)-amino]-butyl}-amino)-propylcarbamoyl]-pyridin-2-yl}-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / 2 h / Reflux

2: triethylamine / tetrahydrofuran / 2 h / 20 °C

With hydrazine hydrate; triethylamine; In tetrahydrofuran;